Liquid Chromatography in Environmental Analysis

Inhaltsverzeichnis

• 1 Quality Assurance in Environmental Trace Analysis.
• 1. The Quality Assurance Program.
• 2. Quality Control Procedures in the Quality Assurance Program.
• 3. Operation of a Quality Assurance Program.
• References.
• 2 Applications of HPLC to the Analysis of Polycyclic Aromatic Hydrocarbons in Environmental Samples.
• 1. Introduction.
• 2. Nomenclature, Structure, and Carcinogenicity.
• 3. Origin and Formation in the Environment.
• 4. Methods of Analysis for Polycyclic Hydrocarbons.
• 5. HPLC Applications in PAH Analysis.
• 6. Conclusions.
• 3 HPLC of Pesticide Residues in Environmental Samples.
• 2. Instrumentation and Methodology.
• 3. Applications.
• 4. Conclusions.
• 4 HPLC Determination of Surfactants and Related Compounds.
• 1. Anionic Surfactants and Related Compounds.
• 2. Nonionic Surfactants.
• 3. Cationic and Amphoteric Surfactants and Related Compounds.
• 5 Trace Metal Analysis by High Performance Liquid Chromatography.
• 2. HPLC—Ultraviolet, —Visible, and/or —Fluorescence Detection of Metal Species.
• 3. HPLC—Mass Spectrometric Detection of Metal Species.
• 4. HPLC—Atomic Absorption Spectroscopic Detection of Metal Species.
• 5. HPLC—Atomic Fluorescence Spectroscopic Detection of Metal Species.
• 6. HPLC—Inductively Coupled or —Direct-Current Plasma Emission Spectroscopic Detection of Metal Species.
• 7. HPLC—Electrochemical and —Conductivity Detection of Metal Species.
• 8. Ion Chromatography—Conductivity Detection of Metal Species.
• 9. Conclusions.
• 6 Anion Analysis by Ion Chromatography.
• 2. Separation Modes.
• 3. Detection Modes.
• 4. New Applications in Anion Ion Chromatography.
• 5. Summary.
• 7 HPLC Sample Injection and Column Switching.
• 1. HPLC Sample Injection Using Valves.
• 2. HPLC Column Switching.
• 8 High Performance Liquid Chromatography as a Cleanup Technique.
• 2. Cleanup for Gas Chromatography (GC) with Electron Capture (EC) or Flame Detection.
• 3. Cleanup for GC—Mass Spectrometry (MS).
• 4. HPLC—HPLC.
• 5. Cleanup for Radioimmunoassay (RIA).
• 6. Radioisotope Fractionation.
• 7. Summary.